rus
Issue #3/2020
I. V. Boldyrev
Measurement Evaluation of the Isotopic Composition Uranium Standards by Total Evaporation Using a Thermal Ionization Mass Spectrometer
Measurement Evaluation of the Isotopic Composition Uranium Standards by Total Evaporation Using a Thermal Ionization Mass Spectrometer
Estimation of the isotopic composition of the fuel is an important task for the nuclear industry. Several basic techniques are known for determining the isotopic composition of heavy elements, such as uranium, both more accurate and longlasting, and express. For production with a large number of samples, the method of total complete evaporation is optimal, providing a high degree of automation and acceptable accuracy of analysis. Total Full evaporation also allows to reduce the qualification level in sample preparation, thereby reducing errors in the results. In this work, standard samples of the composition NBS U010, NBL U030a, and NBL U050 were tested by the method of complete evaporation using a Phoenix thermal ionization mass spectrometer (Isotopx, UK). Statistical processing of the results of a series of experiments showed that, in comparison with others, the total complete evaporation method better meets the accuracy requirements for determining the 235 U/ 238U isotopic ratio and is consistent with published data.
Теги: accreditation administrative code technical regulation testing laboratories административный кодекс аккредитация испытательные лаборатории техническое регулирование
Draft New Code of the Russian Federation on Administrative Violations. Who’s Guilty? And What to Do?
A draft of the new Code of Administrative Offenses of the Russian Federation, prepared by the Ministry of Justice of the Russian Federation published on the website https://regulation.gov.ru/ is discussed. The items of Chapter 24 are examined in detail, which contains “administrative offenses in the field of technical regulation, ensuring the uniformity of measurements, geodesy and cartography, as well as in the field of accreditation in the national accreditation system”. The inconsistency of a number of provisions of the draft Code with the current Law On Technical Regulation and its broad interpretation were noted. Some articles are contrary to the Treaty on the Eurasian Economic Union and other official documents, there are paragraphs that duplicate the articles of the Criminal Code, giving violators the opportunity to evade criminal liability. Changes to some formulations of the CAO RF are proposed, and a number of points, according to the author, should be deleted.
Keywords: administrative code, accreditation, technical regulation, testing laboratories
A draft of the new Code of Administrative Offenses of the Russian Federation, prepared by the Ministry of Justice of the Russian Federation published on the website https://regulation.gov.ru/ is discussed. The items of Chapter 24 are examined in detail, which contains “administrative offenses in the field of technical regulation, ensuring the uniformity of measurements, geodesy and cartography, as well as in the field of accreditation in the national accreditation system”. The inconsistency of a number of provisions of the draft Code with the current Law On Technical Regulation and its broad interpretation were noted. Some articles are contrary to the Treaty on the Eurasian Economic Union and other official documents, there are paragraphs that duplicate the articles of the Criminal Code, giving violators the opportunity to evade criminal liability. Changes to some formulations of the CAO RF are proposed, and a number of points, according to the author, should be deleted.
Keywords: administrative code, accreditation, technical regulation, testing laboratories
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